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Home » GATE Study Material » Chemical Engineering » General Chemical Engineering Concepts » Experienced-Based Rules of Chemical Engineering

Experienced-Based Rules of Chemical Engineering

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Experienced-Based Rules of Chemical Engineering

Cooling Towers

A. With industrial cooling towers, cooling to 90% of the ambient air saturation level is possible.

B. Relative tower size is dependent on the water temperature approach to the wet bulb temperature:

Twater-Twb

Relative Size

5

2.4

15

1.0

25

0.55

C. Water circulation rates are generally 2-4 GPM/sq. ft (81-162 L/min m2) and air velocities are usually 5-7 ft/s
(1.5-2.0 m/s)

D. Countercurrent induced draft towers are the most common. These towers are capable of cooling to within 2 �F
(1.1 �C) of the wet bulb temperature. A 5-10 �F (2.8-5.5 �C) approach is more common.

E. Evaporation losses are about 1% by mass of the circulation rate for every 10 �F (5.5 �C) of cooling. Drift losses are around 0.25% of the circulation rate. A blowdown of about 3% of the circulation rate is needed to prevent salt and chemical treatment buildup.



Conveyors

A. Pneumatic conveyors are best suited for high capacity applications over distances of up to about 400 ft. Pneumatic conveying is also appropriate for multiple sources and destinations. Vacuum or low pressure (6-12 psig or 0.4 to 0.8 bar) is used for generate air velocities from 35 to 120 ft/s (10.7-36.6 m/s). Air requirements are usually in the range of 1 to 7 cubic feet of air per cubic foot of solids (0.03 to 0.5 cubic meters of air per cubic meter of solids).

B. Drag-type conveyors (Redler) are completed enclosed and suited to short distances. Sizes range from 3 to 19 inches square (75 to 480 mm). Travel velocities can be from 30 to 250 ft/min (10 to 75 meters/min). The power requirements for these conveyors is higher than other types.

C. Bucket elevators are generally used for the vertical transport of sticky or abrasive materials. With a bucket measuring 20 in x 20 in (500 mm x 500 mm), capacities of 1000 cubic feet/hr (28 cubic meters/hr) can be reached at speeds of 100 ft/min (30 m/min). Speeds up to 300 ft/min (90 m/min) are possible.

D. Belt conveyors can be used for high capacity and long distance transports. Inclines up to 30� are possible. A 24 in (635 mm) belt can transport 3000 cu. ft./h (85 cu m/h) at speeds of 100 ft/min (30.5 m/min). Speeds can be as high as 600 ft/min (183 m/min). Power consumption is relatively low.

E. Screw conveyors can be used for sticky or abrasive solids for transports up to 150 ft (46 m). Inclines can be up to about 20�. A 12 in (305 mm) diameter screw conveyor can transport 1000-3000 cu. ft./h (28-85 cu. m/h) at around 40-60 rpm.

Crystallization

A. During most crystallizations, C/Csat (concentration/saturated concentration) is kept near 1.02 to 1.05

B. Crystal growth rates and crystal sizes are controlled by limiting the degree of supersaturation.

C. During crystallization by cooling, the temperature of the solution is kept 1-2 �F (0.5-1.2 �C) below the saturation point at the given concentration.

D. A generally acceptable crystal growth rate is 0.10 - 0.80 mm/h

Drivers and Power Recovery

A. Efficiencies: 85-95% for motors, 40-75% for steam turbines, 28-38% for gas engines and turbines.

B. Electric motors are nearly always used for under 100 HP (75 kW). They are available up to 20,000 HP (14,915 kW).

C. Induction motors are most popular. Synchronous motors have speeds as low as 150 rpm at ratings above 50 HP (37.3 kW) only. Synchronous motors are good for low speed reciprocating compressors.

D. Steam turbines are seldom used below 100 HP (75 kW). Their speeds can be controlled and they make good spares for motors in case of a power failure.

E. Gas expanders may be justified for recovering several hundred horsepower. At lower recoveries, pressure let down will most likely be through a throttling valve.

Drying of Solids

A. Spray dryer have drying times of a few seconds. Rotary dryers have drying times ranging from a few minutes to up to an hour.

B. Continuous tray and belt dryers have drying times of 10-200 minutes for granular materials or 3-15 mm pellets.

C. Drum dryers used for highly viscous fluids use contact times of 3-12 seconds and produce flakes 1-3 mm thick. Diameters are generally 1.5-5 ft (0.5 - 1.5 m). Rotation speeds are 2-10 rpm and the maximum evaporation capacity is around 3000 lb/h (1363 kg/h).

D. Rotary cylindrical dryers operate with air velocities of 5-10 ft/s (1.5-3 m/s), up to 35 ft/s (10.5 m/s). Residence times range from 5-90 min. For initial design purposes, an 85% free cross sectional area is used. Countercurrent design should yield an exit gas temperature that is 18-35 �F (10-20 �C) above the solids temperature. Parallel flow should yield an exiting solids temperature of 212 �F (100 �C). Rotation speeds of 4-5 rpm are common. The product of rpm and diameter (in feet) should be 15-25.

E. Pneumatic conveying dryers are appropriate for particles 1-3 mm in diameter and in some cases up to 10 mm. Air velocities are usually 33-100 ft/s (10-30 m/s). Single pass residence time is typically near one minute. Size range from 0.6-1.0 ft (0.2-0.3 m) in diameter by 3.3-125 ft (1-38 m) in length.

F. Fluidized bed dryers work well with particles up to 4.0 mm in diameter. Designing for a gas velocity that is 1.7-2 times the minimum fluidization velocity is good practice. Normally, drying times of 1-2 minutes are sufficient in continuous operation.



Drum Type Vessels

A. Liquid drums are usually horizontal. Gas/Liquid separators are usually vertical

B. Optimum Length/Diameter ratio is usually 3, range is 2.5 to 5

C. Holdup time is 5 minutes for half full reflux drums and gas/liquid separators

Design for a 5-10 minute holdup for drums feeding another column

D. For drums feeding a furnace, a holdup of 30 minutes is a good estimate

E. Knockout drum in front of compressors should be designed for a holdup of

10 times the liquid volume passing per minute.

F. Liquid/Liquid separators should be designed for settling velocities of 2-3 inches/min

G. Gas velocities in gas/liquid separators, velocity = k (liquid density/(vapor density-1))^0.5,

where k is 0.35 with horizontal mesh deentrainers and 0.167 with vertical mesh deentrainers. k is 0.1 without mesh deentrainers and velocity is in ft/s

H. A six inch mesh pad thickness is very popular for such vessels

I. For positive pressure separations, disengagement spaces of 6-18 inches before the mesh pad and 12 inches after the pad are generally suitable.
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